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Grignard Reaction Experiment Part 2 Forming Phenylmagnesium Bromide

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Brant Kedrowski

This organic chemistry lab video describes an experiment where phenyl Grignard reagent is formed from bromobenzene and magnesium metal and then subsequently treated with solid carbon dioxide (CO2) and aqueous acid to synthesize benzoic acid. This product is then separated from a biphenyl impurity using a series of acidbase extractions. The resulting purified benzoic acid is then characterized by IR spectroscopy and melting point analysis. This is the second video in the series and focuses on forming the Grignard reagent, phenylmagnesium bromide.

posted by valeriaangz